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Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial

Received: 22 July 2021     Accepted: 26 August 2021     Published: 4 September 2021
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Abstract

Zinc oxide with neodymium ions nanomaterials were synthesized by using the chemical synthesis method. The materials were characterized by XRD, FTIR, TEM, SEM and spectral analysis. From XRD, TEM and SEM images, the estimated average particle size are 20, 100 and 200nm respectively. Nearly hexagonal shapes for the dark spots in the TEM images indicate that the ZnO nanoparticles are almost hexagonal. SEM demonstrates clearly the formation of cluster type of ZnO nanoparticles and change of the morphology of the nanoparticles with the Nd3+ different ions concentration. UV- Visible absorption spectrum of the ZnO:Nd3+ nanomaterial was analyzed on the basis of Judd-Ofelt (J-O) theory. Nine absorption and four fluorescence bands have been observed at room temperature. Energy interaction and intensity parameters have been computed Fluorescence band have been assigned to transitions 4F3/24I9/2, 4F3/24I11/2, 4F3/24I13/2, and 4F3/24I15/2. The radiative properties were computed using the J-O intensity parameters and fluorescence data. The value of emission cross-section is an important parameter and signifies the rate of energy extraction from the optical material.

Published in American Journal of Nanosciences (Volume 7, Issue 3)
DOI 10.11648/j.ajn.20210703.11
Page(s) 49-53
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2021. Published by Science Publishing Group

Keywords

Absorption and Fluorescence Spectrum, Judd-Ofelt (J-O) Parameters, Radiative Properties

References
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  • APA Style

    Sudha Pal, Yogesh Kumar Sharma, Jitendra Pal Singh. (2021). Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial. American Journal of Nanosciences, 7(3), 49-53. https://doi.org/10.11648/j.ajn.20210703.11

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    ACS Style

    Sudha Pal; Yogesh Kumar Sharma; Jitendra Pal Singh. Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial. Am. J. Nanosci. 2021, 7(3), 49-53. doi: 10.11648/j.ajn.20210703.11

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    AMA Style

    Sudha Pal, Yogesh Kumar Sharma, Jitendra Pal Singh. Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial. Am J Nanosci. 2021;7(3):49-53. doi: 10.11648/j.ajn.20210703.11

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  • @article{10.11648/j.ajn.20210703.11,
      author = {Sudha Pal and Yogesh Kumar Sharma and Jitendra Pal Singh},
      title = {Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial},
      journal = {American Journal of Nanosciences},
      volume = {7},
      number = {3},
      pages = {49-53},
      doi = {10.11648/j.ajn.20210703.11},
      url = {https://doi.org/10.11648/j.ajn.20210703.11},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajn.20210703.11},
      abstract = {Zinc oxide with neodymium ions nanomaterials were synthesized by using the chemical synthesis method. The materials were characterized by XRD, FTIR, TEM, SEM and spectral analysis. From XRD, TEM and SEM images, the estimated average particle size are 20, 100 and 200nm respectively. Nearly hexagonal shapes for the dark spots in the TEM images indicate that the ZnO nanoparticles are almost hexagonal. SEM demonstrates clearly the formation of cluster type of ZnO nanoparticles and change of the morphology of the nanoparticles with the Nd3+ different ions concentration. UV- Visible absorption spectrum of the ZnO:Nd3+ nanomaterial was analyzed on the basis of Judd-Ofelt (J-O) theory. Nine absorption and four fluorescence bands have been observed at room temperature. Energy interaction and intensity parameters have been computed Fluorescence band have been assigned to transitions 4F3/2 → 4I9/2, 4F3/2 →4I11/2, 4F3/2 →4I13/2, and 4F3/2 →4I15/2. The radiative properties were computed using the J-O intensity parameters and fluorescence data. The value of emission cross-section is an important parameter and signifies the rate of energy extraction from the optical material.},
     year = {2021}
    }
    

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  • TY  - JOUR
    T1  - Spectral, Structural and Characterization of NeodymiumIons Doped Zinc Oxide Nanomaterial
    AU  - Sudha Pal
    AU  - Yogesh Kumar Sharma
    AU  - Jitendra Pal Singh
    Y1  - 2021/09/04
    PY  - 2021
    N1  - https://doi.org/10.11648/j.ajn.20210703.11
    DO  - 10.11648/j.ajn.20210703.11
    T2  - American Journal of Nanosciences
    JF  - American Journal of Nanosciences
    JO  - American Journal of Nanosciences
    SP  - 49
    EP  - 53
    PB  - Science Publishing Group
    SN  - 2575-4858
    UR  - https://doi.org/10.11648/j.ajn.20210703.11
    AB  - Zinc oxide with neodymium ions nanomaterials were synthesized by using the chemical synthesis method. The materials were characterized by XRD, FTIR, TEM, SEM and spectral analysis. From XRD, TEM and SEM images, the estimated average particle size are 20, 100 and 200nm respectively. Nearly hexagonal shapes for the dark spots in the TEM images indicate that the ZnO nanoparticles are almost hexagonal. SEM demonstrates clearly the formation of cluster type of ZnO nanoparticles and change of the morphology of the nanoparticles with the Nd3+ different ions concentration. UV- Visible absorption spectrum of the ZnO:Nd3+ nanomaterial was analyzed on the basis of Judd-Ofelt (J-O) theory. Nine absorption and four fluorescence bands have been observed at room temperature. Energy interaction and intensity parameters have been computed Fluorescence band have been assigned to transitions 4F3/2 → 4I9/2, 4F3/2 →4I11/2, 4F3/2 →4I13/2, and 4F3/2 →4I15/2. The radiative properties were computed using the J-O intensity parameters and fluorescence data. The value of emission cross-section is an important parameter and signifies the rate of energy extraction from the optical material.
    VL  - 7
    IS  - 3
    ER  - 

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Author Information
  • Department of Physics, Motiram Baburam Goverment Post Graduate College, Haldwani (Nainital), India

  • Hukum Singh Bora Government Degree College, Someshwar (Almora), India

  • Department of Physics, Sardar Bhagat Singh Government Post Graduate College, Rudrapur (U S Nagar), India

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