In recent nanotechnology is the most promising field for the researchers. This paper describes a simple and convenient procedure for the preparation of crystalline silver nanoparticles. The aggregation of silver nanoparticles was prevented by CH3COONa in a chemical bath and then washed away, leaving crystalline silver nanoparticles. The silver nanoparticles were synthesized by sol-gel technique in the presence of CH3COONa and hydrazine as reducing agent in water at room temperature. The structure and grain size of prepared particles were characterized by Scanning Electron Microscope and X-ray Diffraction. The whole experiment has been carried out at room temperature, using water as solvent and also within very less time. From XRD pattern we got the crystallinity and the position of the crystal plane of the prepared particles was similar to the standard nano silver pattern and the average size of the particles was 11nm. For SEM study it was observed that the particles are homogenous and uniform size in the nano range cracked free surfaces with regular granular shaped grains without any impurities. There was no peak in the carbonyl frequency region confirmed that sodium acetate was not present within the silver particles. From STA study, we have observed that the weight loss was negligible assured the particles were pure. Hence we will describe an excellent scope for large scale production of silver nanocrystals which will have applications in electronics and catalysis.
| Published in | Nanoscience and Nanometrology (Volume 3, Issue 1) |
| DOI | 10.11648/j.nsnm.20170301.16 |
| Page(s) | 34-39 |
| Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
| Copyright |
Copyright © The Author(s), 2017. Published by Science Publishing Group |
Silver Nanoparticles, XRD Technique, FT-IR Spectroscopy, Sol-Gel Technique, SEM Analysis
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APA Style
Mohammad Shahjahan, Md Hasibur Rahman, Mohammad Sajjad Hossain, Most Afroza Khatun, Aminul Islam, et al. (2017). Synthesis and Characterization of Silver Nanoparticles by Sol-Gel Technique. Nanoscience and Nanometrology, 3(1), 34-39. https://doi.org/10.11648/j.nsnm.20170301.16
ACS Style
Mohammad Shahjahan; Md Hasibur Rahman; Mohammad Sajjad Hossain; Most Afroza Khatun; Aminul Islam, et al. Synthesis and Characterization of Silver Nanoparticles by Sol-Gel Technique. Nanosci. Nanometrol. 2017, 3(1), 34-39. doi: 10.11648/j.nsnm.20170301.16
AMA Style
Mohammad Shahjahan, Md Hasibur Rahman, Mohammad Sajjad Hossain, Most Afroza Khatun, Aminul Islam, et al. Synthesis and Characterization of Silver Nanoparticles by Sol-Gel Technique. Nanosci Nanometrol. 2017;3(1):34-39. doi: 10.11648/j.nsnm.20170301.16
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Download@article{10.11648/j.nsnm.20170301.16,
author = {Mohammad Shahjahan and Md Hasibur Rahman and Mohammad Sajjad Hossain and Most Afroza Khatun and Aminul Islam and Most Hosney Ara Begum},
title = {Synthesis and Characterization of Silver Nanoparticles by Sol-Gel Technique},
journal = {Nanoscience and Nanometrology},
volume = {3},
number = {1},
pages = {34-39},
doi = {10.11648/j.nsnm.20170301.16},
url = {https://doi.org/10.11648/j.nsnm.20170301.16},
eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.nsnm.20170301.16},
abstract = {In recent nanotechnology is the most promising field for the researchers. This paper describes a simple and convenient procedure for the preparation of crystalline silver nanoparticles. The aggregation of silver nanoparticles was prevented by CH3COONa in a chemical bath and then washed away, leaving crystalline silver nanoparticles. The silver nanoparticles were synthesized by sol-gel technique in the presence of CH3COONa and hydrazine as reducing agent in water at room temperature. The structure and grain size of prepared particles were characterized by Scanning Electron Microscope and X-ray Diffraction. The whole experiment has been carried out at room temperature, using water as solvent and also within very less time. From XRD pattern we got the crystallinity and the position of the crystal plane of the prepared particles was similar to the standard nano silver pattern and the average size of the particles was 11nm. For SEM study it was observed that the particles are homogenous and uniform size in the nano range cracked free surfaces with regular granular shaped grains without any impurities. There was no peak in the carbonyl frequency region confirmed that sodium acetate was not present within the silver particles. From STA study, we have observed that the weight loss was negligible assured the particles were pure. Hence we will describe an excellent scope for large scale production of silver nanocrystals which will have applications in electronics and catalysis.},
year = {2017}
}
TY - JOUR T1 - Synthesis and Characterization of Silver Nanoparticles by Sol-Gel Technique AU - Mohammad Shahjahan AU - Md Hasibur Rahman AU - Mohammad Sajjad Hossain AU - Most Afroza Khatun AU - Aminul Islam AU - Most Hosney Ara Begum Y1 - 2017/06/30 PY - 2017 N1 - https://doi.org/10.11648/j.nsnm.20170301.16 DO - 10.11648/j.nsnm.20170301.16 T2 - Nanoscience and Nanometrology JF - Nanoscience and Nanometrology JO - Nanoscience and Nanometrology SP - 34 EP - 39 PB - Science Publishing Group SN - 2472-3630 UR - https://doi.org/10.11648/j.nsnm.20170301.16 AB - In recent nanotechnology is the most promising field for the researchers. This paper describes a simple and convenient procedure for the preparation of crystalline silver nanoparticles. The aggregation of silver nanoparticles was prevented by CH3COONa in a chemical bath and then washed away, leaving crystalline silver nanoparticles. The silver nanoparticles were synthesized by sol-gel technique in the presence of CH3COONa and hydrazine as reducing agent in water at room temperature. The structure and grain size of prepared particles were characterized by Scanning Electron Microscope and X-ray Diffraction. The whole experiment has been carried out at room temperature, using water as solvent and also within very less time. From XRD pattern we got the crystallinity and the position of the crystal plane of the prepared particles was similar to the standard nano silver pattern and the average size of the particles was 11nm. For SEM study it was observed that the particles are homogenous and uniform size in the nano range cracked free surfaces with regular granular shaped grains without any impurities. There was no peak in the carbonyl frequency region confirmed that sodium acetate was not present within the silver particles. From STA study, we have observed that the weight loss was negligible assured the particles were pure. Hence we will describe an excellent scope for large scale production of silver nanocrystals which will have applications in electronics and catalysis. VL - 3 IS - 1 ER -
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