Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study

Kismat Ara Elachi; Saddam Hossain; M. M. Haque; Ranjan K. Mohapatra; Kudrat-E-Zahan

doi:doi:10.11648/j.ajmsp.20190401.16

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Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study

Kismat Ara Elachi, Saddam Hossain, M. M. Haque, Ranjan K. Mohapatra, Kudrat-E-Zahan

Published in American Journal of Materials Synthesis and Processing (Volume 4, Issue 1)

Received: 27 May 2019 Accepted: 25 June 2019 Published: 15 July 2019

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Abstract

Four complexes of Cu(II) ions containing Schiff base ligands, L¹ (C₂₀H₁₄O₄N₄) [N,N`-Bis-(2-nitro-benzylidene)-benzene-1,2-diamine] derived from condensation reaction of o-phenylenediamine and 2-nitrobenzaldehyde, L²(C₈H₈N₃SCl)[2-(2-chlorobenzylidene) hydrazinecarbothioamide] derived from condensation reaction of thiosemicarbazide and o-chlorobenzaldehyde and L³(C₉H₁₁N₃OS) [2-(4-methoxybenzylidene)-hydrazinecarbothioamide, derived from the condensation reaction of anisaldehyde and thiosemicarbazide respectively. The synthesized ligands and their metal complexes were isolated in solid state from the reaction medium and characterized by molar conductivity measurement, magnetic susceptibility, infrared, electronic spectral, thermal analysis and some physical measurements. The overall reactions were monitored by TLC analysis.

Published in	American Journal of Materials Synthesis and Processing (Volume 4, Issue 1)
DOI	10.11648/j.ajmsp.20190401.16
Page(s)	43-53
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Schiff Base, Copper Complexes, Antibacterial, Carbazide

References

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APA Style

Kismat Ara Elachi, Saddam Hossain, M. M. Haque, Ranjan K. Mohapatra, Kudrat-E-Zahan. (2019). Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. American Journal of Materials Synthesis and Processing, 4(1), 43-53. https://doi.org/10.11648/j.ajmsp.20190401.16

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ACS Style

Kismat Ara Elachi; Saddam Hossain; M. M. Haque; Ranjan K. Mohapatra; Kudrat-E-Zahan. Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. Am. J. Mater. Synth. Process. 2019, 4(1), 43-53. doi: 10.11648/j.ajmsp.20190401.16

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AMA Style

Kismat Ara Elachi, Saddam Hossain, M. M. Haque, Ranjan K. Mohapatra, Kudrat-E-Zahan. Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. Am J Mater Synth Process. 2019;4(1):43-53. doi: 10.11648/j.ajmsp.20190401.16

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@article{10.11648/j.ajmsp.20190401.16,
  author = {Kismat Ara Elachi and Saddam Hossain and M. M. Haque and Ranjan K. Mohapatra and Kudrat-E-Zahan},
  title = {Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study},
  journal = {American Journal of Materials Synthesis and Processing},
  volume = {4},
  number = {1},
  pages = {43-53},
  doi = {10.11648/j.ajmsp.20190401.16},
  url = {https://doi.org/10.11648/j.ajmsp.20190401.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajmsp.20190401.16},
  abstract = {Four complexes of Cu(II) ions containing Schiff base ligands, L1 (C20H14O4N4) [N,N`-Bis-(2-nitro-benzylidene)-benzene-1,2-diamine] derived from condensation reaction of o-phenylenediamine and 2-nitrobenzaldehyde, L2(C8H8N3SCl)[2-(2-chlorobenzylidene) hydrazinecarbothioamide] derived from condensation reaction of thiosemicarbazide and o-chlorobenzaldehyde and L3(C9H11N3OS) [2-(4-methoxybenzylidene)-hydrazinecarbothioamide, derived from the condensation reaction of anisaldehyde and thiosemicarbazide respectively. The synthesized ligands and their metal complexes were isolated in solid state from the reaction medium and characterized by molar conductivity measurement, magnetic susceptibility, infrared, electronic spectral, thermal analysis and some physical measurements. The overall reactions were monitored by TLC analysis.},
 year = {2019}
}

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TY  - JOUR
T1  - Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study
AU  - Kismat Ara Elachi
AU  - Saddam Hossain
AU  - M. M. Haque
AU  - Ranjan K. Mohapatra
AU  - Kudrat-E-Zahan
Y1  - 2019/07/15
PY  - 2019
N1  - https://doi.org/10.11648/j.ajmsp.20190401.16
DO  - 10.11648/j.ajmsp.20190401.16
T2  - American Journal of Materials Synthesis and Processing
JF  - American Journal of Materials Synthesis and Processing
JO  - American Journal of Materials Synthesis and Processing
SP  - 43
EP  - 53
PB  - Science Publishing Group
SN  - 2575-1530
UR  - https://doi.org/10.11648/j.ajmsp.20190401.16
AB  - Four complexes of Cu(II) ions containing Schiff base ligands, L1 (C20H14O4N4) [N,N`-Bis-(2-nitro-benzylidene)-benzene-1,2-diamine] derived from condensation reaction of o-phenylenediamine and 2-nitrobenzaldehyde, L2(C8H8N3SCl)[2-(2-chlorobenzylidene) hydrazinecarbothioamide] derived from condensation reaction of thiosemicarbazide and o-chlorobenzaldehyde and L3(C9H11N3OS) [2-(4-methoxybenzylidene)-hydrazinecarbothioamide, derived from the condensation reaction of anisaldehyde and thiosemicarbazide respectively. The synthesized ligands and their metal complexes were isolated in solid state from the reaction medium and characterized by molar conductivity measurement, magnetic susceptibility, infrared, electronic spectral, thermal analysis and some physical measurements. The overall reactions were monitored by TLC analysis.
VL  - 4
IS  - 1
ER  -

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Author Information

Kismat Ara Elachi

Department of Chemistry, Universisty of Rajshahi, Rajshahi, Bangladesh
Saddam Hossain

Department of Chemistry, Begum Rokeya University, Rangpur, Bangladesh
M. M. Haque

Department of Chemistry, Universisty of Rajshahi, Rajshahi, Bangladesh
Ranjan K. Mohapatra

Department of Chemistry, Government College of Engineering, Keonjhar, India
Kudrat-E-Zahan

Department of Chemistry, Universisty of Rajshahi, Rajshahi, Bangladesh

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APA Style

Kismat Ara Elachi, Saddam Hossain, M. M. Haque, Ranjan K. Mohapatra, Kudrat-E-Zahan. (2019). Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. American Journal of Materials Synthesis and Processing, 4(1), 43-53. https://doi.org/10.11648/j.ajmsp.20190401.16

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ACS Style

Kismat Ara Elachi; Saddam Hossain; M. M. Haque; Ranjan K. Mohapatra; Kudrat-E-Zahan. Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. Am. J. Mater. Synth. Process. 2019, 4(1), 43-53. doi: 10.11648/j.ajmsp.20190401.16

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AMA Style

Kismat Ara Elachi, Saddam Hossain, M. M. Haque, Ranjan K. Mohapatra, Kudrat-E-Zahan. Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study. Am J Mater Synth Process. 2019;4(1):43-53. doi: 10.11648/j.ajmsp.20190401.16

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@article{10.11648/j.ajmsp.20190401.16,
  author = {Kismat Ara Elachi and Saddam Hossain and M. M. Haque and Ranjan K. Mohapatra and Kudrat-E-Zahan},
  title = {Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study},
  journal = {American Journal of Materials Synthesis and Processing},
  volume = {4},
  number = {1},
  pages = {43-53},
  doi = {10.11648/j.ajmsp.20190401.16},
  url = {https://doi.org/10.11648/j.ajmsp.20190401.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajmsp.20190401.16},
  abstract = {Four complexes of Cu(II) ions containing Schiff base ligands, L1 (C20H14O4N4) [N,N`-Bis-(2-nitro-benzylidene)-benzene-1,2-diamine] derived from condensation reaction of o-phenylenediamine and 2-nitrobenzaldehyde, L2(C8H8N3SCl)[2-(2-chlorobenzylidene) hydrazinecarbothioamide] derived from condensation reaction of thiosemicarbazide and o-chlorobenzaldehyde and L3(C9H11N3OS) [2-(4-methoxybenzylidene)-hydrazinecarbothioamide, derived from the condensation reaction of anisaldehyde and thiosemicarbazide respectively. The synthesized ligands and their metal complexes were isolated in solid state from the reaction medium and characterized by molar conductivity measurement, magnetic susceptibility, infrared, electronic spectral, thermal analysis and some physical measurements. The overall reactions were monitored by TLC analysis.},
 year = {2019}
}

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TY  - JOUR
T1  - Synthesis, Spectral and Thermal Characterization of Cu(II) Complexes Containing Schiff Base Ligands and Their Antibacterial Activity Study
AU  - Kismat Ara Elachi
AU  - Saddam Hossain
AU  - M. M. Haque
AU  - Ranjan K. Mohapatra
AU  - Kudrat-E-Zahan
Y1  - 2019/07/15
PY  - 2019
N1  - https://doi.org/10.11648/j.ajmsp.20190401.16
DO  - 10.11648/j.ajmsp.20190401.16
T2  - American Journal of Materials Synthesis and Processing
JF  - American Journal of Materials Synthesis and Processing
JO  - American Journal of Materials Synthesis and Processing
SP  - 43
EP  - 53
PB  - Science Publishing Group
SN  - 2575-1530
UR  - https://doi.org/10.11648/j.ajmsp.20190401.16
AB  - Four complexes of Cu(II) ions containing Schiff base ligands, L1 (C20H14O4N4) [N,N`-Bis-(2-nitro-benzylidene)-benzene-1,2-diamine] derived from condensation reaction of o-phenylenediamine and 2-nitrobenzaldehyde, L2(C8H8N3SCl)[2-(2-chlorobenzylidene) hydrazinecarbothioamide] derived from condensation reaction of thiosemicarbazide and o-chlorobenzaldehyde and L3(C9H11N3OS) [2-(4-methoxybenzylidene)-hydrazinecarbothioamide, derived from the condensation reaction of anisaldehyde and thiosemicarbazide respectively. The synthesized ligands and their metal complexes were isolated in solid state from the reaction medium and characterized by molar conductivity measurement, magnetic susceptibility, infrared, electronic spectral, thermal analysis and some physical measurements. The overall reactions were monitored by TLC analysis.
VL  - 4
IS  - 1
ER  -

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