Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin

Mahendrasinh Raj; Lata Raj

doi:doi:10.11648/j.ajac.20160403.13

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Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin

Mahendrasinh Raj, Lata Raj

Published in American Journal of Applied Chemistry (Volume 4, Issue 3)

Received: 2 April 2016 Accepted: 12 April 2016 Published: 11 May 2016

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Abstract

Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.

Published in	American Journal of Applied Chemistry (Volume 4, Issue 3)
DOI	10.11648/j.ajac.20160403.13
Page(s)	84-90
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2016. Published by Science Publishing Group

Keywords

Novolac, Resol, Phenolic Oligomer, Mechanical Properties, SEM

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APA Style

Mahendrasinh Raj, Lata Raj. (2016). Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. American Journal of Applied Chemistry, 4(3), 84-90. https://doi.org/10.11648/j.ajac.20160403.13

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ACS Style

Mahendrasinh Raj; Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am. J. Appl. Chem. 2016, 4(3), 84-90. doi: 10.11648/j.ajac.20160403.13

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AMA Style

Mahendrasinh Raj, Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am J Appl Chem. 2016;4(3):84-90. doi: 10.11648/j.ajac.20160403.13

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@article{10.11648/j.ajac.20160403.13,
  author = {Mahendrasinh Raj and Lata Raj},
  title = {Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin},
  journal = {American Journal of Applied Chemistry},
  volume = {4},
  number = {3},
  pages = {84-90},
  doi = {10.11648/j.ajac.20160403.13},
  url = {https://doi.org/10.11648/j.ajac.20160403.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.20160403.13},
  abstract = {Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.},
 year = {2016}
}

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TY  - JOUR
T1  - Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin
AU  - Mahendrasinh Raj
AU  - Lata Raj
Y1  - 2016/05/11
PY  - 2016
N1  - https://doi.org/10.11648/j.ajac.20160403.13
DO  - 10.11648/j.ajac.20160403.13
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 84
EP  - 90
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.20160403.13
AB  - Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.
VL  - 4
IS  - 3
ER  -

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Author Information

Mahendrasinh Raj

Polymer Science & Technology Department, Institute of Science &Technology for Advanced Studies& Research (ISTAR), VallabhVidyanagar, Anand, Gujarat, India
Lata Raj

Chemistry Department, C.N.P.F Arts and D.N Science College, Dabhoi, Vadodara, Gujarat, India

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APA Style

Mahendrasinh Raj, Lata Raj. (2016). Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. American Journal of Applied Chemistry, 4(3), 84-90. https://doi.org/10.11648/j.ajac.20160403.13

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ACS Style

Mahendrasinh Raj; Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am. J. Appl. Chem. 2016, 4(3), 84-90. doi: 10.11648/j.ajac.20160403.13

Copy | Download

AMA Style

Mahendrasinh Raj, Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am J Appl Chem. 2016;4(3):84-90. doi: 10.11648/j.ajac.20160403.13

Copy | Download

@article{10.11648/j.ajac.20160403.13,
  author = {Mahendrasinh Raj and Lata Raj},
  title = {Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin},
  journal = {American Journal of Applied Chemistry},
  volume = {4},
  number = {3},
  pages = {84-90},
  doi = {10.11648/j.ajac.20160403.13},
  url = {https://doi.org/10.11648/j.ajac.20160403.13},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.20160403.13},
  abstract = {Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.},
 year = {2016}
}

Copy | Download

TY  - JOUR
T1  - Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin
AU  - Mahendrasinh Raj
AU  - Lata Raj
Y1  - 2016/05/11
PY  - 2016
N1  - https://doi.org/10.11648/j.ajac.20160403.13
DO  - 10.11648/j.ajac.20160403.13
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 84
EP  - 90
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.20160403.13
AB  - Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.
VL  - 4
IS  - 3
ER  -

Copy | Download